1,5-di-O-tritylxylitol

Base Information

• Chemical Name: 1,5-di-O-tritylxylitol
• CAS No.: 96871-07-7
• Molecular Formula: C₄₃H₄₀O₅
• Molecular Weight: 636.788
• Mol file: 96871-07-7.mol

Synonyms:1,5-di-O-tritylxylitol

Chemical Property of 1,5-di-O-tritylxylitol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,5-di-O-tritylxylitol

There total 9 articles about 1,5-di-O-tritylxylitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

XYLITOL (87-99-0) + trityl chloride (76-83-5) → 1,5-di-O-tritylxylitol (96871-07-7)

Guidance literature:

With pyridine; at 100 ℃; for 21h; Inert atmosphere;

DOI:10.1002/chem.201300533

Reference yield: 85.0%

Adonitol (488-81-3) + trityl chloride (76-83-5) → 1,5-Di-O-trityladonitol (96871-07-7)

Guidance literature:

With pyridine; at 100 ℃; for 22h; Inert atmosphere;

DOI:10.1002/chem.201300533

Reference yield: 67.0%

L-(-)-arabitol (7643-75-6) + trityl chloride (76-83-5) → 1,5-Di-O-trityl-L-arabinitol (96871-07-7)

Guidance literature:

With dmap; triethylamine; In N,N-dimethyl-formamide; for 16h; Ambient temperature;

upstream raw materials:

pyridine

L-(-)-arabitol

trityl chloride

Adonitol

Downstream raw materials:

1,5-O-ditrityl-2,3,4-tri-O-methylribitol

N-Pentyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-L-arabinitol

N-Butyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-L-arabinitol

N-Propyl-2,3,4-tri-O-benzyl-1,5-dideoxy-1,5-imino-L-arabinitol

Refernces

• 1、 Disadee, Wannaporn,Ruchirawat, Somsak. "One-pot cascade synthesis of azabicycles via the nitro-Mannich reaction and N -alkylation". supporting information. p. 707 - 711. Retrieved 2018/02/09.
• 2、 Gallos, John K.,Koftis, Theoharis V.,Karamitrou, Vassiliki I.,Koumbis, Alexandros E.. "Synthesis of cyclitols fused with a furoxan ring from alditols by intramolecular nitrile oxide dimerization". . p. 2461 - 2462. Retrieved 2007/10/03.