2,4-dinitro-benzenesulfonic acid 2-oxo-cyclohexyl ester

Base Information

• Chemical Name: 2,4-dinitro-benzenesulfonic acid 2-oxo-cyclohexyl ester
• CAS No.: 518068-80-9
• Molecular Formula: C₁₂H₁₂N₂O₈S
• Molecular Weight: 344.302
• Mol file: 518068-80-9.mol

Synonyms:2,4-dinitro-benzenesulfonic acid 2-oxo-cyclohexyl ester

Chemical Property of 2,4-dinitro-benzenesulfonic acid 2-oxo-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-dinitro-benzenesulfonic acid 2-oxo-cyclohexyl ester

There total 1 articles about 2,4-dinitro-benzenesulfonic acid 2-oxo-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + hydroxy(phenyl)-λ3-iodanyl 2,4-dinitrobenzenesulfonate (389614-53-3) → 2,4-dinitro-benzenesulfonic acid 2-oxo-cyclohexyl ester (518068-80-9)

Guidance literature:

In acetonitrile; at 80 ℃; for 1h;

DOI:10.1055/s-2002-34236

Reference yield: 95.0%

ethanol (64-17-5) + 2,4-dinitro-benzenesulfonic acid 2-oxo-cyclohexyl ester (518068-80-9) → diethyl adipate (141-28-6)

Guidance literature:

With Oxone; toluene-4-sulfonic acid; at 65 ℃; for 2h;

DOI:10.1055/s-2002-34236

Reference yield: 90.0%

methanol (67-56-1) + 2,4-dinitro-benzenesulfonic acid 2-oxo-cyclohexyl ester (518068-80-9) → hexanedioic acid dimethyl ester (627-93-0)

Guidance literature:

With Oxone; toluene-4-sulfonic acid; at 65 ℃; for 2h;

DOI:10.1055/s-2002-34236

upstream raw materials:

cyclohexanone

hydroxy(phenyl)-λ³-iodanyl 2,4-dinitrobenzenesulfonate

Downstream raw materials:

hexanedioic acid dimethyl ester

diethyl adipate

adipic acid diisopropyl ester

Refernces