Technology Process of Hirsutenone
There total 7 articles about Hirsutenone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; aluminium trichloride;
In
1,2-dichloro-ethane;
for 4h;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / H2 / Pd/C / ethyl acetate / 2 h / 20 °C
2: 33 percent / NaBH4 / methanol / 2 h / 20 °C
3: 84 percent / p-TsOH / benzene / 2 h / Heating
4: 36 percent / AlCl3; pyridine / 1,2-dichloro-ethane / 4 h / Heating
With
pyridine; sodium tetrahydroborate; aluminium trichloride; hydrogen; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
methanol; ethyl acetate; 1,2-dichloro-ethane; benzene;
