4'-O-hexanoylglycitein-7-yl 2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranoside

Base Information

• Chemical Name: 4'-O-hexanoylglycitein-7-yl 2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranoside
• CAS No.: 1105697-69-5
• Molecular Formula: C₃₆H₄₀O₁₅
• Molecular Weight: 712.705
• Mol file: 1105697-69-5.mol

Synonyms:4'-O-hexanoylglycitein-7-yl 2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranoside

Chemical Property of 4'-O-hexanoylglycitein-7-yl 2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4'-O-hexanoylglycitein-7-yl 2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranoside

There total 1 articles about 4'-O-hexanoylglycitein-7-yl 2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

4'-O-hexanoylglycitein (918158-53-9) + 2,3,4,6-tetra-O-acetyl-D-glucopyranosyl 2,2,2-trifluoro-N-(p-methoxyphenyl)acetamidate (1105697-75-3) → 4'-O-hexanoylglycitein-7-yl 2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranoside (1105697-69-5)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 6h; Inert atmosphere; Molecular sieve;

DOI:10.1002/ejoc.200800803

Reference yield: 94.0%

4'-O-hexanoylglycitein-7-yl 2'',3'',4'',6''-tetra-O-acetyl-β-D-glucopyranoside (1105697-69-5) → glycitin (40246-10-4)

Guidance literature:

With water; potassium carbonate; In tetrahydrofuran; methanol; at 40 ℃; for 5h; Inert atmosphere;

DOI:10.1002/ejoc.200800803

upstream raw materials:

4'-O-hexanoylglycitein

2,3,4,6-tetra-O-acetyl-D-glucopyranosyl 2,2,2-trifluoro-N-(p-methoxyphenyl)acetamidate

Downstream raw materials:

glycitin

Refernces