1,10-Dichlorodecane

Base Information

• Chemical Name: 1,10-Dichlorodecane
• CAS No.: 2162-98-3
• Molecular Formula: C10H20Cl2
• Molecular Weight: 211.175
• Hs Code.: 29031980
• European Community (EC) Number: 218-489-6
• NSC Number: 9484
• UNII: 9HLM6UQ45W
• DSSTox Substance ID: DTXSID9062225
• Nikkaji Number: J80.414B
• Wikidata: Q57981763
• Mol file: 2162-98-3.mol

Synonyms:1,10-Dichlorodecane;2162-98-3;Decane, 1,10-dichloro-;Decamethylene dichloride;1,10-dichloro-decane;NSC-9484;C10H20Cl2;NSC9484;Decane,10-dichloro-;1, 10-Dichlorodecane;9HLM6UQ45W;SCHEMBL97813;1,10-Dichlorodecane, 99%;1,10-Decamethylene Dichloride;DTXSID9062225;AMY9370;BCP24948;NSC 9484;EINECS 218-489-6;MFCD00000957;AKOS015915528;DS-4660;CS-0100393;D0247;FT-0606032;D89619;Q-200046;F8881-4366

Chemical Property of 1,10-Dichlorodecane

Chemical Property:

• Appearance/Colour: colourless liquid or white solid
• Vapor Pressure: 0.00515mmHg at 25°C
• Melting Point: 15.6 °C
• Refractive Index: 1.46-1.462
• Boiling Point: 284.3 °C at 760 mmHg
• Flash Point: 108.4 °C
• PSA: 0.00000
• Density: 0.976 g/cm³
• LogP: 4.58480
• Storage Temp.: Store below +30°C.
• Solubility.: Chloroform, Methanol (Slightly)
• XLogP3: 5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 9
• Exact Mass: 210.0942060
• Heavy Atom Count: 12
• Complexity: 64.2

Purity/Quality:

99.9% ^*data from raw suppliers

1,10-Dichlorodecane ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi,N
• Hazard Codes: Xi,N
• Statements: 38-36/37/38-50/53-53
• Safety Statements: 28A-37/39-26-61-60

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C(CCCCCCl)CCCCCl
• Uses: 1,10-Dichlorodecaneis a short-chain chlorinated paraffins (SCCPs), as well as persistent environmental pollutants.

Technology Process of 1,10-Dichlorodecane

There total 20 articles about 1,10-Dichlorodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1,10-decamethylene glycol dichloroformate (56757-75-6) → 1,10-dichlorodecane (2162-98-3)

Guidance literature:

With N,N-dimethyl-formamide; at 130 - 140 ℃;

DOI:10.1021/jo00163a047

Reference yield: 83.0%

1,10-Decanediol (112-47-0) → 1,10-dichlorodecane (2162-98-3)

Guidance literature:

With pyridine; thionyl chloride; for 1h; Heating;

DOI:10.1023/A:1013910404606

Reference yield: 72.0%

(5-chloropentyl)zinc bromide (312624-21-8) → 1,10-dichlorodecane (2162-98-3)

Guidance literature:

With Desyl chloride; dichloro[2,2'-bis(diphenylphosphino)-1,1'-binaphthyl]palladium(II); In tetrahydrofuran; at 20 ℃;

DOI:10.1021/ol0258536

upstream raw materials:

1,10-Decanediol

6-chlorohexanoic acid

1,5,5,6,6,10-hexachloro-decane

1,5,6,10-tetrachloro-dec-5-ene

Downstream raw materials:

dodecanebis(thiolic)acid S,S-diphenyl ester

1,12-Diaminododecane

1,10-bis(trichlorosilyl)decane

Refernces

• 1、 Buchina, I. K.,Kholbekov, O. Kh.,Abduvakhabov, A. A.. "DETECTION AND SYNTHESIS OF A SYNERGIST OF THE SEX PHEROMONE OF THE COTTON BOLLWORM". . p. 121 - 123. Retrieved 1994.
• 2、 Sakai, Norio,Nakajima, Takumi,Yoneda, Shinichiro,Konakahara, Takeo,Ogiwara, Yohei. "Gallium-catalyzed reductive chlorination of carboxylic acids with copper(II) chloride". . p. 10619 - 10623. Retrieved 2015/02/19.
• 3、 Sokolov,Turovskii,Lukevits. "The synthesis of phosphates of long-chain ω-hydroxyalkyl esters of 11-deoxyprostaglandin E1". . p. 62 - 64. Retrieved 2007/10/03.