Ethanamine, N-ethyl-, acetate

Base Information

• Chemical Name: Ethanamine, N-ethyl-, acetate
• CAS No.: 20726-63-0
• Deprecated CAS: 856328-31-9
• Molecular Formula: C6H15NO2
• Molecular Weight: 133.191
• Hs Code.: 2921199090
• European Community (EC) Number: 243-990-1
• DSSTox Substance ID: DTXSID2066646
• Mol file: 20726-63-0.mol

Synonyms:diethylamine;diethylamine acetate;diethylamine hydrobromide;diethylamine hydrochloride;diethylamine perchlorate;diethylamine phosphate (1:1);diethylamine sulfate;diethylamine sulfite (1:1)

Chemical Property of Ethanamine, N-ethyl-, acetate

Chemical Property:

• Melting Point: 47 °C
• Boiling Point: 55.5oC
• PSA: 49.33000
• LogP: 1.09760
• Water Solubility.: within almost transparency
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 133.110278721
• Heavy Atom Count: 9
• Complexity: 42.1

Purity/Quality:

98%,99%, ^*data from raw suppliers

Diethylamine Acetate >97.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: Nitrogen Compounds -> Amines, Aliphatic
• Canonical SMILES: CCNCC.CC(=O)O

Technology Process of Ethanamine, N-ethyl-, acetate

There total 5 articles about Ethanamine, N-ethyl-, acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

S,S-diethyl-N-diethylamidodithiophosphite (42964-63-6) + acetic acid (64-19-7,77671-22-8) → N,N-diethylamine acetate (20726-63-0) + O-acetyl S,S-diethyl phosphorodithioite (84103-76-4)

Guidance literature:

for 1h; Ambient temperature;

Reference yield: 78.0%

O-acetyl S,S-diethyl phosphorodithioite (84103-76-4) + diethylamine (109-89-7) → S,S-diethyl-N-diethylamidodithiophosphite (42964-63-6) + N,N-diethylamine acetate (20726-63-0)

Guidance literature:

In diethyl ether; at 0 ℃;

Reference yield: 64.0%

dipropyl diethylphosphoramidodithioite (53431-44-0) + acetic acid (64-19-7,77671-22-8) → N,N-diethylamine acetate (20726-63-0)

Guidance literature:

for 1h; Ambient temperature;

upstream raw materials:

S,S-diethyl-N-diethylamidodithiophosphite

acetic acid

dipropyl diethylphosphoramidodithioite

O-acetyl S,S-diethyl phosphorodithioite

Refernces

• 1、 Attri, Pankaj,Reddy, P. Madhusudan,Venkatesu,Kumar, Anil,Hofman. "Measurements and molecular interactions for N, N-dimethylformamide with ionic liquid mixed solvents". . p. 6126 - 6133. Retrieved 2010.
• 2、 Govinda, Varadhi,Attri, Pankaj,Venkatesu,Venkateswarlu. "Temperature effect on the molecular interactions between two ammonium ionic liquids and dimethylsulfoxide". . p. 218 - 225. Retrieved 2011.
• 3、 Sun, Xuejun,Cao, Bobo,Zhou, Xinming,Liu, Shuangyue,Zhu, Xiao,Fu, Hu. "Theoretical and experimental studies on proton transfer in acetate-based protic ionic liquids". . p. 254 - 261. Retrieved 2016/07/06.