9,10-Dihydro-9,10-dioxo-1,4-anthracenedisulfonic acid

Base Information

• Chemical Name: 9,10-Dihydro-9,10-dioxo-1,4-anthracenedisulfonic acid
• CAS No.: 14486-59-0
• Molecular Formula: C₁₄H₈O₈S₂
• Molecular Weight: 368.345
• Mol file: 14486-59-0.mol

Synonyms:9,10-Dihydro-9,10-dioxo-1,4-anthracenedisulfonic acid;9,10-Dihydro-9,10-dioxoanthracene-1,4-disulfonic acid

Chemical Property of 9,10-Dihydro-9,10-dioxo-1,4-anthracenedisulfonic acid

Chemical Property:

• Melting Point: 262 °C (decomp)(Solv: water (7732-18-5))
• PKA: -2.60±0.20(Predicted)
• Density: 1.800±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9,10-Dihydro-9,10-dioxo-1,4-anthracenedisulfonic acid

There total 6 articles about 9,10-Dihydro-9,10-dioxo-1,4-anthracenedisulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9,10-dioxo-9,10-dihydro-anthracene-1,4-disulfenyl chloride (100526-83-8) → 1,4-Anthrachinondisulfonsaeure (14486-59-0)

Guidance literature:

With chlorine; acetic acid;

DOI:10.1021/ja01569a043

Reference yield:

1-Nitro-4-chloroanthraquinone (6337-82-2) → 1,4-Anthrachinondisulfonsaeure (14486-59-0)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous dioxane; Na₂S_.9H₂O / Behandeln des Reaktionsprodukts mit Chlor in CHCl₃ unter Zusatz von Aluminium

2: aqueous acetic acid; chlorine

With 1,4-dioxane; sodium sulfide; chlorine; acetic acid;

DOI:10.1021/ja01569a043

Reference yield:

9,10-dioxo-9,10-dihydro-anthracene-1,4-disulfenic acid dimethyl ester (409314-32-5) → 1,4-Anthrachinondisulfonsaeure (14486-59-0)

Guidance literature:

With chlorine; acetic acid;

DOI:10.1021/ja01569a043

upstream raw materials:

1,4-dichloroanthraquinone

9,10-dioxo-9,10-dihydro-anthracene-1,4-disulfenyl chloride

9,10-dioxo-9,10-dihydro-anthracene-1,4-disulfenic acid

9,10-dioxo-9,10-dihydro-anthracene-1,4-disulfenic acid dimethyl ester