DISPERSE VIOLET 17

Base Information

• Chemical Name: DISPERSE VIOLET 17
• CAS No.: 12217-92-4
• Molecular Formula: C14H8BrNO3
• Molecular Weight: 318.12222
• Mol file: 12217-92-4.mol

Synonyms:Red Violet 17

Chemical Property of DISPERSE VIOLET 17

Chemical Property:

• PSA: 80.39000
• LogP: 3.09350

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DISPERSE VIOLET 17

There total 15 articles about DISPERSE VIOLET 17 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-hydroxy-1-aminoanthraquinone (116-85-8) → 1-amino-2-bromo-4-hydroxyanthraquinone (116-82-5,12217-92-4)

Guidance literature:

With bromine; at 50 - 60 ℃; Bio-ionic liquid;

DOI:10.1039/b923589b

Reference yield: 89.5%

1-amino-9,10-anthracenedione (82-45-1) → 1-amino-2-bromo-4-hydroxyanthraquinone (116-82-5,12217-92-4)

Guidance literature:

With bromine; boric acid; In water;

Reference yield: 86.6%

→ 1-amino-2-bromo-4-hydroxyanthraquinone (116-82-5,12217-92-4) + 1-amino-4-hydroxy-2-chloroanthraquinone (2478-67-3)

Guidance literature:

upstream raw materials:

1-amino-2, 4-dibromoanthraquinone

4-hydroxy-1-aminoanthraquinone

1-amino-4-methoxyanthraquinone

1-amino-2-bromo-4-phenoxy-9,10-antraquinone

Downstream raw materials:

N-[4-(1-Amino-4-hydroxy-9,10-dioxo-9,10-dihydro-anthracen-2-yloxy)-3-methyl-phenyl]-acetamide

N-[3-(1-Amino-4-hydroxy-9,10-dioxo-9,10-dihydro-anthracen-2-yloxy)-4-chloro-phenyl]-acetamide

1-[3-(1-Amino-4-hydroxy-9,10-dioxo-9,10-dihydro-anthracen-2-yloxy)-phenyl]-3-phenyl-urea

N-[4-(1-Amino-4-hydroxy-9,10-dioxo-9,10-dihydro-anthracen-2-yloxy)-phenyl]-acetamide

Refernces

• 1、 Phadtare, Sunanda Balaso,Shankarling, Ganapati Subray. "Halogenation reactions in biodegradable solvent: Efficient bromination of substituted 1-aminoanthra-9,10-quinone in deep eutectic solvent (choline chloride:urea)". experimental part. p. 458 - 462. Retrieved 2010/08/07.
• 2、 -. "Process for the preparation of a mixture of 1-amino-2-chloro-4-hydroxyanthraquinone and 1-amino-2-bromo-4-hydroxyanthraquinone". . . Retrieved 2008/06/13.