Technology Process of 3-CHLORO-2,6-DIFLUOROPHENYLACETIC ACID
There total 4 articles about 3-CHLORO-2,6-DIFLUOROPHENYLACETIC ACID which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; potassium hydroxide;
at 110 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triphenylphosphine; carbon tetrabromide / dichloromethane / 2 h / 20 °C
2: ethanol / 2 h / 85 °C
3: water; potassium hydroxide / 3 h / 110 °C
With
carbon tetrabromide; water; triphenylphosphine; potassium hydroxide;
In
ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 20 °C
2: triphenylphosphine; carbon tetrabromide / dichloromethane / 2 h / 20 °C
3: ethanol / 2 h / 85 °C
4: water; potassium hydroxide / 3 h / 110 °C
With
carbon tetrabromide; dimethylsulfide borane complex; water; triphenylphosphine; potassium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane;
