N-[1,1'-biphenyl]-4-yl-N-(4-bromophenyl)-9,9-dimethyl-9H-Fluoren-2-amine

Base Information Edit

Chemical Name:N-[1,1'-biphenyl]-4-yl-N-(4-bromophenyl)-9,9-dimethyl-9H-Fluoren-2-amine
CAS No.:1246562-40-2
Molecular Formula:C33H26BrN
Molecular Weight:516.48
Hs Code.:
Mol file:1246562-40-2.mol

Synonyms:N-(4-bromophenyl)-9,9-dimethyl-N-(4-phenylphenyl)fluoren-2-amine;2-Amino-N-[(1,1'-biphenyl)-4-yl]-N-(4-bromophenyl)-9,9-dimethylfluorene;

Suppliers and Price of N-[1,1'-biphenyl]-4-yl-N-(4-bromophenyl)-9,9-dimethyl-9H-Fluoren-2-amine

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
2-Amino-N-[(1,1'-biphenyl)-4-yl]-N-(4-bromophenyl)-9,9-dimethylfluorene >98.0%(HPLC)(N)
1g
$ 38.00

TCI Chemical
2-Amino-N-[(1,1'-biphenyl)-4-yl]-N-(4-bromophenyl)-9,9-dimethylfluorene >98.0%(HPLC)(N)
5g
$ 165.00

Matrix Scientific
N-([1,1'-Biphenyl]-4-yl)-N-(4-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine 95+%
250mg
$ 545.00

Matrix Scientific
N-([1,1'-Biphenyl]-4-yl)-N-(4-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine 95+%
1g
$ 1210.00

Crysdot
N-([1,1'-Biphenyl]-4-yl)-N-(4-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine 95+%
100g
$ 986.00

Crysdot
N-([1,1'-Biphenyl]-4-yl)-N-(4-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine 95+%
25g
$ 493.00

Crysdot
N-([1,1'-Biphenyl]-4-yl)-N-(4-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine 95+%
10g
$ 248.00

Arctom
N-([1,1'-Biphenyl]-4-yl)-N-(4-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine 95%
10g
$ 81.00

Arctom
N-([1,1'-Biphenyl]-4-yl)-N-(4-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine 95%
1g
$ 15.00

Arctom
N-([1,1'-Biphenyl]-4-yl)-N-(4-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine 95%
5g
$ 50.00

Total 90 raw suppliers

Chemical Property of N-[1,1'-biphenyl]-4-yl-N-(4-bromophenyl)-9,9-dimethyl-9H-Fluoren-2-amine Edit

Chemical Property:

Melting Point:159.0 to 163.0 °C
Boiling Point:655.9±55.0 °C(Predicted)
PKA:-3.55±0.40(Predicted)
PSA：3.24000
Density:1.293±0.06 g/cm3 (20 oC 760 Torr), Calc.*
LogP:9.89220
Storage Temp.:Keep in dark place,Sealed in dry,Room Temperature
Solubility.:soluble in Tetrahydrofuran

Purity/Quality:

99.0% ^*data from raw suppliers

2-Amino-N-[(1,1'-biphenyl)-4-yl]-N-(4-bromophenyl)-9,9-dimethylfluorene >98.0%(HPLC)(N) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses N-([1,1''-Biphenyl]-4-yl)-N-(4-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine is used as a reactant in the synthesis of novel hole transport materials for efficient green electroluminescent devices.

Technology Process of N-[1,1'-biphenyl]-4-yl-N-(4-bromophenyl)-9,9-dimethyl-9H-Fluoren-2-amine

There total 8 articles about N-[1,1'-biphenyl]-4-yl-N-(4-bromophenyl)-9,9-dimethyl-9H-Fluoren-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1246562-40-2
biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenylamine

Guidance literature:: With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate; In toluene; for 13h; Reflux;

Reference yield: 91.8%

: 897671-69-1
N?(biphenyl?4?yl)?9,9?dimethyl?9H?fluorene?2?amine

: 589-87-7
1,4-bromoiodobenzene

: 1246562-40-2
biphenyl-4-yl-(9,9-dimethyl-9H-fluoren-2-yl)-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenylamine

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; potassium hydroxide; In o-xylene; water; at 150 ℃; for 8h; Inert atmosphere;
DOI:10.1016/j.tet.2017.06.031