Cinnamaldehyde Diethylacetal

Base Information

• Chemical Name: Cinnamaldehyde Diethylacetal
• CAS No.: 7148-78-9
• Molecular Formula: C13H18O2
• Molecular Weight: 206.285
• Mol file: 7148-78-9.mol

Synonyms:Cinnamaldehyde Diethylacetal;SCHEMBL3276111;3,3-diethoxyl-1-phenylprop-1-ene;FT-0636366

Chemical Property of Cinnamaldehyde Diethylacetal

Chemical Property:

• Appearance/Colour: colorless transparent liquid
• Vapor Pressure: 0.00236mmHg at 25°C
• Refractive Index: 1.524
• Boiling Point: 297.6 °C at 760 mmHg
• Flash Point: 110.1 °C
• PSA: 18.46000
• Density: 0.984 g/cm³
• LogP: 3.09890
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 206.130679813
• Heavy Atom Count: 15
• Complexity: 165

Purity/Quality:

99.9% ^*data from raw suppliers

CinnamaldehydeDiethylAcetal ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(C=CC1=CC=CC=C1)OCC

Technology Process of Cinnamaldehyde Diethylacetal

There total 17 articles about Cinnamaldehyde Diethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

orthoformic acid triethyl ester (122-51-0) + 3-phenyl-propenal (104-55-2) → 3,3-diethoxyl-1-phenylprop-1-ene (7148-78-9)

Guidance literature:

With N-Bromosuccinimide; In ethanol; at 20 ℃; for 0.25h;

Reference yield: 95.0%

ethanol (64-17-5) + 2-styryl-1,3-oxathiolane (80563-94-6) → 3,3-diethoxyl-1-phenylprop-1-ene (7148-78-9)

Guidance literature:

With N-Bromosuccinimide; at 20 ℃; for 0.166667h;

DOI:10.1016/S0040-4020(02)00389-7

Reference yield: 85.0%

triethoxyantimony (873376-62-6) + 3-phenyl-propenal (104-55-2) → 3,3-diethoxyl-1-phenylprop-1-ene (7148-78-9)

Guidance literature:

With allyl bromide; at 80 ℃; for 4h;

DOI:10.1039/c39900000493

upstream raw materials:

phenylpropargyl aldehyde diethyl acetal

orthoformic acid triethyl ester

3-phenyl-propenal

ethanol

Downstream raw materials:

(2E,6E)-5-Ethoxy-7-phenyl-hepta-2,6-dienal

2-styryl-1,3-dithiolane

6-nitro-2-phenyl chromene epoxide

6-cyano-2-phenyl-3,4-epoxy-chromene

Refernces

• 1、 Hou, Junying,Luan, Yi,Huang, Xiubing,Gao, Hongyi,Yang, Mu,Lu, Yunfeng. "Facile synthesis of Cu3(BTC)2/cellulose acetate mixed matrix membranes and their catalytic applications in continuous flow process". . p. 9123 - 9129. Retrieved 2017/08/29.
• 2、 Bulman Page, Philip C.,Appleby, Louise F.,Chan, Yohan,Day, David P.,Buckley, Benjamin R.,Slawin, Alexandra M. Z.,Allin, Steven M.,McKenzie, Michael J.. "Kinetic resolution in asymmetric epoxidation using iminium salt catalysis". . p. 8074 - 8082. Retrieved 2013/09/12.