sapindoside B

Base Information

• Chemical Name: sapindoside B
• CAS No.: 30994-75-3
• Molecular Formula: C₄₆H₇₄O₁₆
• Molecular Weight: 883.084
• Mol file: 30994-75-3.mol

Synonyms:SapindosideB (8CI);Akebia saponin PG;Kalopanaxsaponin I;Prosapogenin CP5;

Chemical Property of sapindoside B

Chemical Property:

• Boiling Point: 975.1°Cat760mmHg
• Flash Point: 280.8°C
• Density: 1.38g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of sapindoside B

There total 26 articles about sapindoside B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

hederagenin 3-O-(3,4-di-O-acetyl-α-L-arabinopyranosyl)-(1->3)-α-L-rhamnopyranosyl-(1->2)-4-O-acetyl-α-L-arabinopyranoside (1157918-38-1) → hederagenin?3?O?[β?D?xylopyranosyl?(1→3)]?[α?L?rhamnopyranosyl?(1→2)]?α?L?arabinopyranoside (29321-28-6,30994-75-3,72629-76-6,80666-65-5)

Guidance literature:

With methanol; sodium methylate; at 20 ℃; for 3h;

DOI:10.1248/cpb.57.198

Reference yield:

hederagenin-3-O-β-D-xylopyranosyl-(1->3)-O-α-L-rhamnopyranosyl-(1->2)-O-α-L-arabinopyranosyl-28-O-α-L-rhamnopyranosyl-(1->4)-O-β-D-glucopyranosyl-(1->6)-O-β-D-glucopyranosyl ester (119742-55-1) → hedaragenin (465-99-6) + prosapogenin (17184-21-3) + sapindoside B (29321-28-6,72629-76-6,80666-65-5,30994-75-3) + alpha-Hederin (27013-91-8)

Guidance literature:

With Bacteroides JY-6; Bifidobacterium K-111; In various solvent(s); at 37 ℃; for 36h;

DOI:10.1248/bpb.21.360

Reference yield:

3-O-β-D-xylopyranosyl(1->3)-α-L-rhamnopyranosyl(1->2)-α-L-arabinopyranosyl hederagenin 28-O-β-D-xylopyranosyl(1->4)-β-D-glycopyranosyl(1->6)-β-D-glycopyranoside → hedaragenin (465-99-6) + sapindoside B (29321-28-6,72629-76-6,80666-65-5,30994-75-3)

Guidance literature:

With hydrogenchloride; In ethanol; for 0.666667h; Heating;

upstream raw materials:

methanol

mukurozisaponin Y₁

hederagenin 3-O-β-D-glucopyranosyl-(1-4)-β-D-xylopyranosyl-(1-3)-α-L-rhamnopyranosyl-(1-2)-α-L-arabinopyranoside

hederagenin 3-O-β-D-glucopyranosyl-(1-4)-β-D-glucopyranosyl-(1-4)-β-D-xylopyranosyl-(1-3)-α-L-rhamnopyranosyl-(1-2)-α-L-arabinopyranoside

Downstream raw materials:

D-Xylose

L-rhamnose

L-(+)-arabinose

hederagenin

Refernces

• 1、 Asao, Yasunobu,Morikawa, Toshio,Yuanyuan,Okamoto, Masaki,Hamao, Makoto,Matsuda, Hisashi,Muraoka, Osamu,Yuan, Dan,Yoshikawa, Masayuki. "Structures of acetylated oleanane-type triterpene saponins, rarasaponins IV, V, and VI, and anti-Hyperlipidemic constituents from the pericarps of sapindus rarak". experimental part. p. 198 - 203. Retrieved 2009/09/25.
• 2、 Panov,Grishkovets,Kachala,Shashkov. "Triterpene glycosides from Kalopanax septemlobum. II. Glycosides E, K, and L from leaves of Kalopanax septemlobum var. maximowiczii introduced to Crimea". . p. 322 - 325. Retrieved 2008/02/01.