14-deoxyandrographoside

Base Information

• Chemical Name: 14-deoxyandrographoside
• CAS No.: 82209-72-1
• Molecular Formula: C₂₆H₄₀O₉
• Molecular Weight: 496.598
• Mol file: 82209-72-1.mol

Synonyms:2(5H)-Furanone,3-[2-[5-[(b-D-glucopyranosyloxy)methyl]decahydro-6-hydroxy-5,8a-dimethyl-2-methylene-1-naphthalenyl]ethyl]-,[1R-(1a,4ab,5a,6a,8aa)]-; Andropanoside; Ninandrographolide

Chemical Property of 14-deoxyandrographoside

Chemical Property:

• Vapor Pressure: 5.98E-23mmHg at 25°C
• Boiling Point: 704.6°C at 760 mmHg
• Flash Point: 232.7°C
• PSA: 145.91000
• Density: 1.32g/cm³
• LogP: 0.81600

Purity/Quality:

98% ^*data from raw suppliers

Andropanoside 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 14-deoxyandrographoside

There total 1 articles about 14-deoxyandrographoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

UDP-glucose (133-89-1) + 14-deoxyandrographolide (4176-97-0) → 14-deoxyandrographolide 19-glucoside (82209-72-1)

Guidance literature:

With glucosyltransferase from Andrographis paniculata; In aq. buffer; at 30 ℃; for 12h; pH=7.4; Kinetics; Enzymatic reaction;

DOI:10.1021/acs.orglett.8b02146

Reference yield: 2.0%

14-deoxyandrographolide 19-glucoside (82209-72-1) → 14-deoxyandrographolide (4176-97-0)

Guidance literature:

With acetate buffer; β-glucosidase; at 36 ℃; for 50h; pH=4.95;

Reference yield:

14-deoxyandrographolide 19-glucoside (82209-72-1) → iso-14-deoxyandrographolide (79233-15-1)

Guidance literature:

With hydrogenchloride; In ethanol; at 100 ℃; for 4h; sealed tube;

upstream raw materials:

UDP-glucose

14-deoxyandrographolide

Downstream raw materials:

14-deoxyandrographolide

iso-14-deoxyandrographolide

Refernces