1,26-Hexacosanediol

Base Information

• Chemical Name: 1,26-Hexacosanediol
• CAS No.: 15541-01-2
• Molecular Formula: C26H54O2
• DSSTox Substance ID: DTXSID20587782
• Metabolomics Workbench ID: 47399
• Nikkaji Number: J2.719.770A
• Wikidata: Q82480283
• Mol file: 15541-01-2.mol

Synonyms:1,26-Hexacosanediol;HEXACOSANE-1,26-DIOL;15541-01-2;SCHEMBL10772196;DTXSID20587782;LMFA05000581

Chemical Property of 1,26-Hexacosanediol

Chemical Property:

• XLogP3: 11.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 25
• Exact Mass: 398.412380961
• Heavy Atom Count: 28
• Complexity: 229

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CCCCCCCCCCCCCO)CCCCCCCCCCCCO

Technology Process of 1,26-Hexacosanediol

There total 18 articles about 1,26-Hexacosanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

hexacosa-1,25-diene (103043-51-2) → hexacosane-1,26-diol (15541-01-2)

Guidance literature:

hexacosa-1,25-diene; With diisoamyl borane; In tetrahydrofuran; at 20 ℃;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; ethanol; at 50 ℃; for 3h; Further stages.;

DOI:10.1002/chem.200601866

Reference yield: 79.0%

hexacosanedioic acid dimethyl ester (86797-43-5) → hexacosane-1,26-diol (15541-01-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 6h; Inert atmosphere; Reflux;

DOI:10.1021/jacs.1c08031

Reference yield:

hexacosa-4,10,16,22-tetrayne-1,26-diol (96074-35-0) → hexacosane-1,26-diol (15541-01-2)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethyl acetate; Ambient temperature;

DOI:10.1021/jo01067a023

upstream raw materials:

hexacosanedioic acid diethyl ester

hexacosa-4,10,16,22-tetrayne-1,26-diol

hexacosa-1,25-diene

1,13-tridecanediol

Refernces

• 1、 Staiger, Anne,Paren, Benjamin A.,Zunker, Robin,Hoang, Son,H?u?ler, Manuel,Winey, Karen I.,Mecking, Stefan. "Anhydrous Proton Transport within Phosphonic Acid Layers in Monodisperse Telechelic Polyethylenes". supporting information. p. 16725 - 16733. Retrieved 2021/10/21.