Technology Process of 2,4-DIHYDROXY-6-METHYLBENZOIC ACID ETHYL ESTER
There total 30 articles about 2,4-DIHYDROXY-6-METHYLBENZOIC ACID ETHYL ESTER which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
sodium hydroxide;
for 15h;
under 760 Torr;
Ambient temperature;
- Guidance literature:
-
ethyl acetoacetate;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 20 ℃;
Inert atmosphere;
With
n-butyllithium;
In
tetrahydrofuran; hexane; mineral oil;
for 10h;
Inert atmosphere;
DOI:10.1016/j.bmcl.2021.128410