Di((2H3)methyl)ammonium chloride

Base Information

• Chemical Name: Di((2H3)methyl)ammonium chloride
• CAS No.: 53170-19-7
• Molecular Formula: C2H2ClD6N
• Molecular Weight: 87.4976
• Hs Code.: 28459000
• European Community (EC) Number: 258-409-7
• DSSTox Substance ID: DTXSID40201236
• Mol file: 53170-19-7.mol

Synonyms:53170-19-7;Di((2H3)methyl)ammonium chloride;Dimethylamine-d6 Hydrochloride;Dimethylamine D6 Hydrochloride;DIMETHYL-D 6-AMINE HYDROCHLORIDE;Dimethyl-d6-amine hydrochloride;EINECS 258-409-7;Dimethyl-d6 amine hydrochloride;1,1,1-trideuterio-N-(trideuteriomethyl)methanamine;hydrochloride;C2H8ClN;DTXSID40201236;BCP22198;Deuterated dimethylamine hydrochloride;MFCD00064544;AKOS015894778;AT12613;DI((2)H?)METHYLAMINE HYDROCHLORIDE;Dimethyl-d6-amine hydrochloride, 99 atom % D;A934854

Chemical Property of Di((2H3)methyl)ammonium chloride

Chemical Property:

• Vapor Pressure: 322mmHg at 25°C
• Melting Point: 170-173 °C (lit.)
• Boiling Point: 47 °C at 760 mmHg
• PSA: 12.03000
• LogP: 1.02850
• Sensitive.: Hygroscopic
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 87.0721874
• Heavy Atom Count: 4
• Complexity: 2.8

Purity/Quality:

99% ^*data from raw suppliers

Dimethylamine-d6 Hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn, Xi
• Hazard Codes: Xn,Xi
• Statements: 22-36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CNC.Cl
• Isomeric SMILES: [2H]C([2H])([2H])NC([2H])([2H])[2H].Cl

Technology Process of Di((2H3)methyl)ammonium chloride

There total 6 articles about Di((2H3)methyl)ammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C9H7(2)H6N*ClH → d6-dimethylamine hydrochloride (53170-19-7)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In methanol; ethanol; at 40 ℃;

Reference yield: 71.0%

C10H7(2)H6NO2 → d6-dimethylamine hydrochloride (53170-19-7)

Guidance literature:

With hydrogenchloride; palladium on activated charcoal; hydrogen; In methanol; water; at 20 ℃;

Reference yield: 70.0%

N-trideuteromethyl carbamate → d6-dimethylamine hydrochloride (53170-19-7)

Guidance literature:

With hydrogenchloride; palladium on activated charcoal; In methanol; water; at 20 ℃;

upstream raw materials:

N-nitrosodimethylamine-d₆

N,N-Bis-(D₃-methyl)-p-toluolsulfonamid

Downstream raw materials:

1-(4-chloro-2-iodophenyl)-3,3-dimethyl-d6-triazene

[²H₆]SKandF-S-104864

[2H₆,34S]-4-nitrophenyl-S,N,N-dimethyl thiocarbamate

3-(3,4-dichlorophenyl)-1,1-bis(methyl-D3)urea

Refernces

• 1、 Liu, Zhaogang,Ren, Xiangyu,Wang, Peng. "A practical synthesis of deuterated methylamine and dimethylamine". . p. 265 - 268. Retrieved 2020/11/30.
• 2、 -. "Method for synthesizing deuterated dimethylamine salt with deuterated methanol". Paragraph 0025-0026; 0031-0032. . Retrieved 2020/07/12.