tetracyclo[6.1.0.0~2,4~.0~5,7~]nonane

Base Information Edit

Chemical Name:tetracyclo[6.1.0.0~2,4~.0~5,7~]nonane
CAS No.:37831-90-6
Molecular Formula:C9H12
Molecular Weight:120.194
Hs Code.:2902199090
Mol file:37831-90-6.mol

Synonyms:3,6-endomethylene-1,2,3,6-tetrahydrophtaloyl chloride;endo,exo-bicyclo[2,2,1]-hept-5-ene-2,3-dicarboxylic acid chloride;3,6-ENDOMETHYLENE-1,2,3,6-TETRAHYDROPHTHALOYL CHLORIDE;TRANS-3,6-ENDO-METHYLENE-1,2,3,6-TETRAHYDROPHTHALOYL CHLORIDE;trans-bicyclo[2.2.1]hept-5-ene-2,3-dicarbonyl dichloride;trans-bicyclo(2.2.1)hept-5-enyl-2,3-dicarbonylchloride;endo,exo-bishomobarrelene;endo,exo-bicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid dichloride;endo,exo-bicyclo[2.2.1]hept-2-ene-5,6-dicarboxylic acid dichloride;trans-5-norbornene-3-dicarbonylchloride;(2-endo,3-exo)-bicyclo[2.2.1]hept-5-ene-2,3-dicarbonyl dichloride;5-NORBORNENE-2,3-DICARBONYL CHLORIDE;endo,exo-Tetracyclo<6.1.0.02,4.05,7>nonan;endo,exo-norbornene-2,3-dicarboxylic acid dichloride;endo,exo-Dihomobarrelene;(+/-)-trans-norborn-5-ene-2,3-dicarbonyl dichloride;BICYCLO[2.2.1]-5-HEPTENE-2,3-DICARBONYL CHLORIDE;

Suppliers and Price of tetracyclo[6.1.0.0~2,4~.0~5,7~]nonane

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetracyclo[6.1.0.0~2,4~.0~5,7~]nonane Edit

Chemical Property:

Vapor Pressure:3.07mmHg at 25°C
Boiling Point:160.7°Cat760mmHg
Flash Point:28°C
PSA：0.00000
Density:1.169g/cm³
LogP:1.90830

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tetracyclo[6.1.0.0~2,4~.0~5,7~]nonane

There total 2 articles about tetracyclo[6.1.0.0~2,4~.0~5,7~]nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 75-11-6
diiodomethane

: 3786-99-0,58342-05-5
cis-transoid-cis-tricyclo<5,1,0,0>-oct-5-ene

: 37831-90-6
endo,exo-Tetracyclo<6.1.0.0^2,4.0^5,7>nonan

Guidance literature:: With diethylzinc; In diethyl ether; for 24h; Heating;

Reference yield:

: 66563-21-1
C₁₅H₁₈N₂O₂S

: 37831-90-6
endo,exo-Tetracyclo<6.1.0.0^2,4.0^5,7>nonan

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 2M MeLi / diethyl ether / 15 h / Ambient temperature

2: 45 percent / ZnEt₂ / diethyl ether / 24 h / Heating

With methyllithium; diethylzinc; In diethyl ether;