SODIUM DEUTEROXIDE

Base Information

• Chemical Name: SODIUM DEUTEROXIDE
• CAS No.: 14014-06-3
• Molecular Formula: DNa O
• Molecular Weight: 40.9892
• Hs Code.: 28459000
• Mol file: 14014-06-3.mol

Synonyms:Deuteratedsodium hydroxide; Sodium deuteroxide; Sodium deuteroxide (NaOD); Sodiumhydroxide-d

Chemical Property of SODIUM DEUTEROXIDE

Chemical Property:

• Appearance/Colour: colourless solution
• Vapor Pressure: 24.5mmHg at 25°C
• Refractive Index: n20/D 1.4196
• Boiling Point: 100°Cat760mmHg
• Flash Point: °C
• PSA: 23.06000
• Density: g/cm³
• LogP: -0.17680
• Sensitive.: Air & Moisture Sensitive
• Water Solubility.: Fully miscible in water.

Purity/Quality:

99% ^*data from raw suppliers

SodiumDeuteroxide(40%w/winD2O) ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 35-34-20/21/22
• Safety Statements: 26-36/37/39-45-27-23

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Uses: Sodium deuteroxide is a reagent used in the synthesis of rac Zearalenone-d6. is used in many chemical reactions and industrial practices.

Technology Process of SODIUM DEUTEROXIDE

There total 7 articles about SODIUM DEUTEROXIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

water-d2 (7789-20-0) + sodium (7440-23-5) → deuteriated sodium hydroxide (14014-06-3)

Guidance literature:

In neat (no solvent); D2O vapor;;

Reference yield:

water-d2 (7789-20-0) + sodium hydroxide (1310-73-2) → deuteriated sodium hydroxide (14014-06-3)

Guidance literature:

In water-d2; complete isotope exchange on dissolving NaOH in D2O;;

Reference yield:

water-d2 (7789-20-0) → deuteriated sodium hydroxide (14014-06-3)

Guidance literature:

With sodium; In toluene; metallic Na was dissolved in D2O under toluene in a separatory funnel;

upstream raw materials:

water-d2

sodium

sodium hydroxide

deuterium

Downstream raw materials:

[PdCl(PPh₂CD=CBu(t)NN=CBu(t)CD₂PPh₂)]

[PdCl(PPh₂CD=CBu(t)NN=CBu(t)CH₂PPh₂)]

[PtCl(PPh₂CD=CBu(t)NN=CBu(t)CD₂PPh₂)]

[PtCl(PPh₂CD=CBu(t)NN=CBu(t)CH₂PPh₂)]

Refernces

• 1、 Bruchanan, R. A.. "". . p. 870 - 874. Retrieved 1959.
• 2、 Guella,Zanchetta,Patton,Miotello. "New insights on the mechanism of palladium-catalyzed hydrolysis of sodium borohydride from11B NMR measurements". . p. 17024 - 17033. Retrieved 2008/10/09.
• 3、 Evans,O'Hare,Clement. "The structure of Co(η-C5H5)2+ and NMe4+ intercalates of MnPS3: An X-ray, neutron-diffraction, and solid-state NMR study". . p. 4595 - 4606. Retrieved 2007/10/02.