16,28-Secosolanid-5-ene-3,16-diol, (3beta,16beta,22alpha,25beta)-

Base Information Edit

Chemical Name:16,28-Secosolanid-5-ene-3,16-diol, (3beta,16beta,22alpha,25beta)-
CAS No.:6785-55-3
Molecular Formula:C27H45NO2
Molecular Weight:415.66
Hs Code.:
Mol file:6785-55-3.mol

Synonyms:Dihydrosolasodenol;Solaverbascine;(22S,25R)-16,28-seco-solanid-5-ene-3β,16β-diol;(22S,25R)-16,28-Seco-solanid-5-en-3β,16β-diol;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 16,28-Secosolanid-5-ene-3,16-diol, (3beta,16beta,22alpha,25beta)- Edit

Chemical Property:

Vapor Pressure:4.09E-14mmHg at 25°C
Melting Point:208.5-210.5 °C
Boiling Point:544.2°Cat760mmHg
PKA:15.01±0.70(Predicted)
Flash Point:59°C
PSA：52.49000
Density:1.09g/cm³
LogP:5.25010

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 16,28-Secosolanid-5-ene-3,16-diol, (3beta,16beta,22alpha,25beta)-

There total 33 articles about 16,28-Secosolanid-5-ene-3,16-diol, (3beta,16beta,22alpha,25beta)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35410-24-3
(22R,25S)-22,26-Epiminocholest-5-ene-3β,16β-diol

: 1176-36-9,6785-55-3,35410-24-3,36456-16-3,65027-00-1,65027-01-2,68422-03-7,96391-23-0,123123-41-1
(3S,8S,9S,10R,13S,14S,17R)-10,13-Dimethyl-17-[(S)-1-((2S,5S)-5-methyl-piperidin-2-yl)-ethyl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene-3,16-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NaHCO₃ / H₂O; toluene / 20 h / Ambient temperature

2: 63 percent / CrO₃, NaOAc*3H₂O, AcOH / H₂O / 20 h / Ambient temperature

3: 290 mg / Na, i-PrOH / toluene / 2.5 h / Heating

With chromium(VI) oxide; sodium acetate; sodium; sodium hydrogencarbonate; acetic acid; isopropyl alcohol; In water; toluene;

Reference yield:

: 4847-09-0,129850-55-1,129938-49-4,129938-51-8,129938-52-9
(3S,8S,9S,10R,13S,14S,17R)-17-[(S)-1-((2S,5S)-1-Chloro-5-methyl-piperidin-2-yl)-ethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene-3,16-diol

: 1176-36-9,6785-55-3,35410-24-3,36456-16-3,65027-00-1,65027-01-2,68422-03-7,96391-23-0,123123-41-1
(3S,8S,9S,10R,13S,14S,17R)-10,13-Dimethyl-17-[(S)-1-((2S,5S)-5-methyl-piperidin-2-yl)-ethyl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene-3,16-diol

Guidance literature:: Multi-step reaction with 5 steps

1: 31 percent / NaOMe / methanol / 2 h / Heating

2: NaBH₄ / methanol / Ambient temperature

3: 98 percent / NaHCO₃ / H₂O; toluene / 20 h / Ambient temperature

4: 63 percent / CrO₃, NaOAc*3H₂O, AcOH / H₂O / 20 h / Ambient temperature

5: 290 mg / Na, i-PrOH / toluene / 2.5 h / Heating

With chromium(VI) oxide; sodium tetrahydroborate; sodium methylate; sodium acetate; sodium; sodium hydrogencarbonate; acetic acid; isopropyl alcohol; In methanol; water; toluene;

Reference yield:

: 546-40-7
(25S)-3β-hydroxy-22βN-spirosol-5-ene

: 1176-36-9,6785-55-3,35410-24-3,36456-16-3,65027-00-1,65027-01-2,68422-03-7,96391-23-0,123123-41-1
(3S,8S,9S,10R,13S,14S,17R)-10,13-Dimethyl-17-[(S)-1-((2S,5S)-5-methyl-piperidin-2-yl)-ethyl]-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene-3,16-diol

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / methanol / Ambient temperature

2: 98 percent / NaHCO₃ / H₂O; toluene / 20 h / Ambient temperature

3: 63 percent / CrO₃, NaOAc*3H₂O, AcOH / H₂O / 20 h / Ambient temperature

4: 290 mg / Na, i-PrOH / toluene / 2.5 h / Heating

With chromium(VI) oxide; sodium tetrahydroborate; sodium acetate; sodium; sodium hydrogencarbonate; acetic acid; isopropyl alcohol; In methanol; water; toluene;