4-(6-Hydroxyhexyloxy)benzaldehyde

Base Information

• Chemical Name: 4-(6-Hydroxyhexyloxy)benzaldehyde
• CAS No.: 96735-91-0
• Molecular Formula: C13H18O3
• Molecular Weight: 222.284
• DSSTox Substance ID: DTXSID50567572
• Nikkaji Number: J1.192.681I
• Wikidata: Q72484359
• Mol file: 96735-91-0.mol

Synonyms:4-(6-hydroxyhexyloxy)benzaldehyde;96735-91-0;SCHEMBL2222324;DTXSID50567572;YCKLLCWNZUJZHZ-UHFFFAOYSA-N;4-(6-Hydroxyhexyloxy)-benzaldehyde;4-(6-Hydroxy-hexyloxy)-benzaldehyde;4-[(6-HYDROXYHEXYL)OXY]BENZALDEHYDE

Chemical Property of 4-(6-Hydroxyhexyloxy)benzaldehyde

Chemical Property:

• XLogP3: 2.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 8
• Exact Mass: 222.125594432
• Heavy Atom Count: 16
• Complexity: 174

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C=O)OCCCCCCO

Technology Process of 4-(6-Hydroxyhexyloxy)benzaldehyde

There total 5 articles about 4-(6-Hydroxyhexyloxy)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

6-chloro-1-hexanol (2009-83-8) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 4-(6-hydroxyhexyl-1-oxy)benzaldehyde (96735-91-0)

Guidance literature:

With caesium carbonate; In acetonitrile; at 85 ℃; for 12h;

DOI:10.1039/c9cc07919j

Reference yield: 87.0%

1-iodohexan-6-ol (40145-10-6) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 4-(6-hydroxyhexyl-1-oxy)benzaldehyde (96735-91-0)

Guidance literature:

With potassium carbonate; In acetonitrile; at 100 ℃; for 14h; Inert atmosphere;

DOI:10.1002/anie.201107104

Reference yield: 81.0%

1-bromo-6-hexanol (4286-55-9) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 4-(6-hydroxyhexyl-1-oxy)benzaldehyde (96735-91-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 10h;

DOI:10.1039/d0tc04832a

upstream raw materials:

6-chloro-1-hexanol

4-hydroxy-benzaldehyde

1-bromo-6-hexanol

1-iodohexan-6-ol

Downstream raw materials:

1'-methyl-2'-[4-(6-hydroxyhexyloxy)phenyl]-2',3',4',5'-tetrahydropyrrolo[3',4':1,2][60]fullerene

4-(6-p-tosyloxy)hexyloxybenzaldehyde

C₁₃H₁₆O₃

C₇₇H₁₀₁N₃O₁₂

Refernces

• 1、 Qiu, Shuai,Gao, Zhao,Yan, Fei,Yuan, Hongxing,Wang, Jingxia,Tian, Wei. "1,8-Dioxapyrene-based electrofluorochromic supramolecular hyperbranched polymers". supporting information. p. 383 - 386. Retrieved 2020/01/11.
• 2、 -. "Liquid crystal aligning, liquid crystal alignment film, the liquid crystal display element and manufacturing method of the liquid crystal display element, and polymerizable compound". Page/Page column 70; 71. . Retrieved 2016/10/08.