Technology Process of Canniprene
There total 24 articles about Canniprene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium; butan-1-ol;
- Guidance literature:
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Multi-step reaction with 6 steps
1: 71 percent / pyridine / 22 h
2: 97 percent / H2 / 10percent palladium on carbon / ethyl acetate / 16 h / 20 °C
3: 24 percent / potassium carbonate, potassium iodide, 18-crown-6 / acetone / 22 h / Heating
4: H2 / Lindlar catalyst / ethyl acetate / 0.33 h / 20 °C
5: 40 mg / 1.25 h / 150 °C
6: 90 percent / aqueous 10percent sodium hydroxide, ethanol / 1 h / 85 °C
With
pyridine; sodium hydroxide; 18-crown-6 ether; ethanol; hydrogen; potassium carbonate; potassium iodide;
palladium on activated charcoal; Lindlar's catalyst;
In
ethyl acetate; acetone;
