Technology Process of 4-Phenyl-2,3-dihydro-1h-inden-1-one
There total 7 articles about 4-Phenyl-2,3-dihydro-1h-inden-1-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate;
In
1,4-dioxane; water;
at 80 ℃;
Inert atmosphere;
DOI:10.1021/acs.orglett.0c03651
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
ethanol; water; toluene;
at 110 ℃;
Schlenk technique;
Inert atmosphere;
Sealed tube;
With
dihydrogen peroxide;
In
ethanol; water; toluene;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / 1 h / Reflux
2: aluminum (III) chloride / carbon disulfide / 2.5 h / Reflux
3: tris-imidazolium-stabilized palladium; potassium carbonate / water; toluene / 22 h / 90 °C
With
aluminum (III) chloride; thionyl chloride; tris-imidazolium-stabilized palladium; potassium carbonate;
In
carbon disulfide; water; toluene;
3: Suzuki coupling;
DOI:10.1002/adsc.201100574