Propanoic acid, 3-[(4-methoxyphenyl)methoxy]-, (5Z,8Z)-5,8-tetradecadienyl ester

Base Information Edit

Chemical Name:Propanoic acid, 3-[(4-methoxyphenyl)methoxy]-, (5Z,8Z)-5,8-tetradecadienyl ester
CAS No.:392333-42-5
Molecular Formula:C₂₅H₃₈O₄
Molecular Weight:402.574
Hs Code.:
Mol file:392333-42-5.mol

Synonyms:

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Chemical Property of Propanoic acid, 3-[(4-methoxyphenyl)methoxy]-, (5Z,8Z)-5,8-tetradecadienyl ester Edit

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Technology Process of Propanoic acid, 3-[(4-methoxyphenyl)methoxy]-, (5Z,8Z)-5,8-tetradecadienyl ester

There total 11 articles about Propanoic acid, 3-[(4-methoxyphenyl)methoxy]-, (5Z,8Z)-5,8-tetradecadienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31333-13-8
3-nonyn-1-ol

: 392333-42-5
3-(4-Methoxy-benzyloxy)-propionic acid (5Z,8Z)-tetradeca-5,8-dienyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / Lindlar catalyst / ethanol

2.1: 85 percent / I₂; imidazole; triphenylphosphine / acetonitrile; diethyl ether / 0.75 h / 20 °C

3.1: 6 g / acetonitrile / 48 h / 60 °C

4.1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 2 h / 0 °C

4.2: TsOH / methanol / 1 h / 20 °C

5.1: DCC; DMAP / CH₂Cl₂ / 3 h / 20 °C

With 1H-imidazole; dmap; n-butyllithium; hydrogen; iodine; dicyclohexyl-carbodiimide; triphenylphosphine; Lindlar's catalyst; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; hexane; dichloromethane; acetonitrile;
DOI:10.1016/S0957-4166(01)00381-0

Reference yield:

: 110-53-2
1-Bromopentane

: 392333-42-5
3-(4-Methoxy-benzyloxy)-propionic acid (5Z,8Z)-tetradeca-5,8-dienyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: 70 percent / lithium amide / liquid ammonia; tetrahydrofuran; hexamethylphosphoric acid triamide / 6 h

2.1: hydrogen / Lindlar catalyst / ethanol

3.1: 85 percent / I₂; imidazole; triphenylphosphine / acetonitrile; diethyl ether / 0.75 h / 20 °C

4.1: 6 g / acetonitrile / 48 h / 60 °C

5.1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 2 h / 0 °C

5.2: TsOH / methanol / 1 h / 20 °C

6.1: DCC; DMAP / CH₂Cl₂ / 3 h / 20 °C

With 1H-imidazole; dmap; n-butyllithium; lithium amide; hydrogen; iodine; dicyclohexyl-carbodiimide; triphenylphosphine; Lindlar's catalyst; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; hexane; dichloromethane; ammonia; acetonitrile;
DOI:10.1016/S0957-4166(01)00381-0