Butanoic acid, 4-[(4-methoxyphenyl)methoxy]-, (4Z,7Z)-4,7-tridecadienyl ester

Base Information Edit

Chemical Name:Butanoic acid, 4-[(4-methoxyphenyl)methoxy]-, (4Z,7Z)-4,7-tridecadienyl ester
CAS No.:356790-00-6
Molecular Formula:C₂₅H₃₈O₄
Molecular Weight:402.574
Hs Code.:
Mol file:356790-00-6.mol

Synonyms:

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Chemical Property of Butanoic acid, 4-[(4-methoxyphenyl)methoxy]-, (4Z,7Z)-4,7-tridecadienyl ester Edit

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Technology Process of Butanoic acid, 4-[(4-methoxyphenyl)methoxy]-, (4Z,7Z)-4,7-tridecadienyl ester

There total 9 articles about Butanoic acid, 4-[(4-methoxyphenyl)methoxy]-, (4Z,7Z)-4,7-tridecadienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31333-13-8
3-nonyn-1-ol

: 356790-00-6
4-(4-Methoxy-benzyloxy)-butyric acid (4Z,7Z)-trideca-4,7-dienyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / Lindlar catalyst / ethanol

2.1: 85 percent / I₂; imidazole; triphenylphosphine / acetonitrile; diethyl ether / 0.75 h / 20 °C

3.1: 6 g / acetonitrile / 48 h / 60 °C

4.1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 2 h / 0 °C

4.2: TsOH / methanol / 1 h / 20 °C

5.1: DCC; DMAP / CH₂Cl₂ / 3 h / 20 °C

With 1H-imidazole; dmap; n-butyllithium; hydrogen; iodine; dicyclohexyl-carbodiimide; triphenylphosphine; Lindlar's catalyst; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; hexane; dichloromethane; acetonitrile;
DOI:10.1016/S0957-4166(01)00381-0

Reference yield:

: 110-53-2
1-Bromopentane

: 356790-00-6
4-(4-Methoxy-benzyloxy)-butyric acid (4Z,7Z)-trideca-4,7-dienyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: 70 percent / lithium amide / liquid ammonia; tetrahydrofuran; hexamethylphosphoric acid triamide / 6 h

2.1: hydrogen / Lindlar catalyst / ethanol

3.1: 85 percent / I₂; imidazole; triphenylphosphine / acetonitrile; diethyl ether / 0.75 h / 20 °C

4.1: 6 g / acetonitrile / 48 h / 60 °C

5.1: n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide; hexane / 2 h / 0 °C

5.2: TsOH / methanol / 1 h / 20 °C

6.1: DCC; DMAP / CH₂Cl₂ / 3 h / 20 °C

With 1H-imidazole; dmap; n-butyllithium; lithium amide; hydrogen; iodine; dicyclohexyl-carbodiimide; triphenylphosphine; Lindlar's catalyst; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; hexane; dichloromethane; ammonia; acetonitrile;
DOI:10.1016/S0957-4166(01)00381-0