N,N'-DIMETHYL-1,8-OCTANEDIAMINE

Base Information

• Chemical Name: N,N'-DIMETHYL-1,8-OCTANEDIAMINE
• CAS No.: 33563-54-1
• Molecular Formula: C10H24N2
• Molecular Weight: 172.31100
• Hs Code.: 2921290000
• Mol file: 33563-54-1.mol

Synonyms:N,N-Dimethyl-1,8-octamethylendiamin;N,N'-Dimethyl-1,8-diamino-octan;N,N'-dimethyl-1,8-diaminooctane;N,N inverted exclamation marka-Dimethyl-1,8-octanediamine;N,N'-Dimethyl-1,8-octanediamine;N,N'-Dimethyl-oktamethylendiamin;1,8-Octanediamine,N,N'-dimethyl;

Chemical Property of N,N'-DIMETHYL-1,8-OCTANEDIAMINE

Chemical Property:

• Melting Point: 31-36oC(lit.)
• Refractive Index: 1.4300 (estimate)
• Boiling Point: 249oC(lit.)
• Flash Point: 215 °F
• PSA: 24.06000
• Density: 0.769 g/mL at 25oC(lit.)
• LogP: 2.54760

Purity/Quality:

99% ^*data from raw suppliers

N,N′-Dimethyl-1,8-octanediamine 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of N,N'-DIMETHYL-1,8-OCTANEDIAMINE

There total 7 articles about N,N'-DIMETHYL-1,8-OCTANEDIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,8-diaminooctan (373-44-4) → N,N'-dimethyloctane-1,8-diamine (33563-54-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Heating

2: LiAlH₄

With lithium aluminium tetrahydride;

DOI:10.1021/jo034092x

Reference yield:

dimethyl octane-1,8-diyldicarbamate (6580-86-5) → N,N'-dimethyloctane-1,8-diamine (33563-54-1)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.1021/jm00322a018

Reference yield:

C24H34N2(2+)*2CH3O4S(1-) (75190-02-2) → N,N'-dimethyloctane-1,8-diamine (33563-54-1)

Guidance literature:

With sulfuric acid; In water; for 1h; Yield given; Heating;

upstream raw materials:

dimethyl octane-1,8-diyldicarbamate

NN'-di(benzylidene)-1,8-diaminooctane

dimethyl sulfate

C₂₄H₃₄N₂⁽²⁺⁾*2CH₃O₄S^(1-)

Downstream raw materials:

Ni(C₁₂H₁₄N₄(CH₃)2(C(C₆H₅)NH(CH₂)8NHC(C₆H₅)))⁽²⁺⁾*2PF₆^(1-)=(Ni(C₃₆H₄₈N₆))(PF₆)2

N,N'-bis<6-<<(benzyloxy)carbonyl>amino>caproyl>-N,N'-dimethyl-1,8-octanediamine

Refernces

• 1、 Denmark, Scott E.,Pham, Son M.. "Stereoselective aldol additions of achiral ethyl ketone-derived trichlorosilyl enolates". . p. 5045 - 5055. Retrieved 2007/10/03.