Tetrahedron Letters p. 415 - 418 (1998)
Update date:2022-08-11
Topics:
Liu, Meizheng
Yu, Biao
Hui, Yongzheng
The first total synthesis of 25(R)-ruscogenin-1-yl β-D-xylopyranosyl-(1→3)-[β-D-glucopyranosyl-(1→2)]-β-D-fucopyranoside (1), an Ophiopogonis saponin with strong anti-inflammatory and immunopharmacological activities from the tuber of Liriope muscari (Decne.), is described. The glycosylation of a highly hindered alcohol by Schmidt's 'inverse procedure' is demonstrated.
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